1 Ocak 2018 Dergi makalesi Açık Erişim

Armutcu, Canan; Uzun, Lokman; Denizli, Adil

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        "affiliation": "Hacettepe Univ, Dept Chem, Ankara, Turkey", 
        "name": "Armutcu, Canan"
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      {
        "affiliation": "Hacettepe Univ, Dept Chem, Ankara, Turkey", 
        "name": "Uzun, Lokman"
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      {
        "affiliation": "Hacettepe Univ, Dept Chem, Ankara, Turkey", 
        "name": "Denizli, Adil"
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    "description": "Automated on-line two-dimensional high-performance liquid chromatography method (2D-HPLC) is proposed to determine Ochratoxin A (OTA) in food samples as an alternative to OTA immunoaffinity column (IAC). An on-line 2D-HPLC system is designed for the analysis of OTA using an affinity-based monolithic column in the first dimension and reversed-phase C18 column in the second dimension. Initially, optimal OTA separation efficiency is determined through traditional HPLC system consisting of a P(HEMAPA) monolithic column coupled with HPLC system. Secondly, after providing optimum conditions, OTA determination was investigated through the 2D-HPLC system. According to results, 2D-HPLC system showed good linearity in the range 0.5 to 20 ng/mL with limit of detection (LOD) and limit of quantification (LOQ) values of 21.2 pg/mL and 64.3 pg/mL, respectively. The P(HEMAPA)-4 monolithic column displayed good recovery of OTA ranging from 104.34% to 107.33%. Relative standard deviations (RSD) varied in the range 0.21% to 1.31% thus indicating the efficiency of P(HEMAPA)-4 monolithic column developed for OTA. (C) 2018 Elsevier B.V. All rights reserved.", 
    "doi": "10.1016/j.chroma.2018.07.057", 
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    "journal": {
      "pages": "139-148", 
      "title": "JOURNAL OF CHROMATOGRAPHY A", 
      "volume": "1569"
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    "title": "Determination of Ochratoxin A traces in foodstuffs: Comparison of an automated on-line two-dimensional high-performance liquid chromatography and off-line immunoaffinity-high-performance liquid chromatography system"
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