Dergi makalesi Açık Erişim
Kublay, Irem Zehra; Kocoglu, Elif Seda; Oflu, Sude; Arvas, Busra; Yolacan, Cigdem; Bakirdere, Sezgin
{ "@context": "https://schema.org/", "@id": 269168, "@type": "ScholarlyArticle", "creator": [ { "@type": "Person", "affiliation": "Yildiz Tech Univ, Fac Art & Sci, Chem Dept, TR-34220 Istanbul, Turkiye", "name": "Kublay, Irem Zehra" }, { "@type": "Person", "affiliation": "Yildiz Tech Univ, Cent Res Lab, TR-34220 Istanbul, Turkiye", "name": "Kocoglu, Elif Seda" }, { "@type": "Person", "affiliation": "Yildiz Tech Univ, Fac Art & Sci, Chem Dept, TR-34220 Istanbul, Turkiye", "name": "Oflu, Sude" }, { "@type": "Person", "affiliation": "Yildiz Tech Univ, Fac Art & Sci, Chem Dept, TR-34220 Istanbul, Turkiye", "name": "Arvas, Busra" }, { "@type": "Person", "affiliation": "Yildiz Tech Univ, Fac Art & Sci, Chem Dept, TR-34220 Istanbul, Turkiye", "name": "Yolacan, Cigdem" }, { "@type": "Person", "name": "Bakirdere, Sezgin" } ], "datePublished": "2023-01-01", "description": "<p>In order to eliminate the effects of seawater matrix on the precise/accurate determination of elements, new and efficient analytical procedure requires. In this study, co-precipitation method based on the triethylamine (TEA)-assisted Mg(OH)(2) was performed to eliminate side-effects of seawater medium on the determination with flame atomic absorption spectrometry (FAAS) prior to the preconcentration of nickel by an optimized dispersive liquid-liquid microextraction (DLLME) method. Under the optimum conditions of the presented method, the limit of detection and quantification (LOD, LOQ) values obtained for nickel were found as 16.1 and 53.8 & mu;g kg(-1), respectively. Seawater samples collected from West Antarctic region were used for real sample applications to check the accuracy and applicability of developed method, and satisfying recovery results (86-97%) were obtained. In addition to this, the digital image-based colorimetric detection system and the UV-Vis system were applied to confirm the applicability of the developed DLLME-FAAS method in other analytical systems.</p>", "headline": "Trace nickel determination in seawater matrix using combination of dispersive liquid-liquid microextraction and triethylamine-assisted Mg(OH)<sub>2</sub> method", "identifier": 269168, "image": "https://aperta.ulakbim.gov.tr/static/img/logo/aperta_logo_with_icon.svg", "license": "http://www.opendefinition.org/licenses/cc-by", "name": "Trace nickel determination in seawater matrix using combination of dispersive liquid-liquid microextraction and triethylamine-assisted Mg(OH)<sub>2</sub> method", "url": "https://aperta.ulakbim.gov.tr/record/269168" }
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