1 Ocak 2023 Dergi makalesi Açık Erişim

Kublay, Irem Zehra; Kocoglu, Elif Seda; Oflu, Sude; Arvas, Busra; Yolacan, Cigdem; Bakirdere, Sezgin

Citation Style Language JSON

{
  "DOI": "10.1007/s10661-023-11435-y", 
  "abstract": "<p>In order to eliminate the effects of seawater matrix on the precise/accurate determination of elements, new and efficient analytical procedure requires. In this study, co-precipitation method based on the triethylamine (TEA)-assisted Mg(OH)(2) was performed to eliminate side-effects of seawater medium on the determination with flame atomic absorption spectrometry (FAAS) prior to the preconcentration of nickel by an optimized dispersive liquid-liquid microextraction (DLLME) method. Under the optimum conditions of the presented method, the limit of detection and quantification (LOD, LOQ) values obtained for nickel were found as 16.1 and 53.8 &amp; mu;g kg(-1), respectively. Seawater samples collected from West Antarctic region were used for real sample applications to check the accuracy and applicability of developed method, and satisfying recovery results (86-97%) were obtained. In addition to this, the digital image-based colorimetric detection system and the UV-Vis system were applied to confirm the applicability of the developed DLLME-FAAS method in other analytical systems.</p>", 
  "author": [
    {
      "family": "Kublay", 
      "given": " Irem Zehra"
    }, 
    {
      "family": "Kocoglu", 
      "given": " Elif Seda"
    }, 
    {
      "family": "Oflu", 
      "given": " Sude"
    }, 
    {
      "family": "Arvas", 
      "given": " Busra"
    }, 
    {
      "family": "Yolacan", 
      "given": " Cigdem"
    }, 
    {
      "family": "Bakirdere", 
      "given": " Sezgin"
    }
  ], 
  "container_title": "ENVIRONMENTAL MONITORING AND ASSESSMENT", 
  "id": "269168", 
  "issue": "7", 
  "issued": {
    "date-parts": [
      [
        2023, 
        1, 
        1
      ]
    ]
  }, 
  "page": "10", 
  "title": "Trace nickel determination in seawater matrix using combination of dispersive liquid-liquid microextraction and triethylamine-assisted Mg(OH)<sub>2</sub> method", 
  "type": "article-journal", 
  "volume": "195"
}