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Resolution of (+/-)-beta-Methylphenylethylamine by a Novel Chiral Stationary Phase for Pirkle-Type Column Chromatography

Yilmaz, Hayrullah; Topal, Giray; Cakmak, Resit; Hosgoren, Halil


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<oai_dc:dc xmlns:dc="http://purl.org/dc/elements/1.1/" xmlns:oai_dc="http://www.openarchives.org/OAI/2.0/oai_dc/" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.openarchives.org/OAI/2.0/oai_dc/ http://www.openarchives.org/OAI/2.0/oai_dc.xsd">
  <dc:creator>Yilmaz, Hayrullah</dc:creator>
  <dc:creator>Topal, Giray</dc:creator>
  <dc:creator>Cakmak, Resit</dc:creator>
  <dc:creator>Hosgoren, Halil</dc:creator>
  <dc:date>2010-01-01</dc:date>
  <dc:description>In this study, a new Pirkle-type chiral column stationary phase for resolution of beta-methylphenylethyl amine was described by using activated Sepharose 4B as a matrix, L-tyrosine as a spacer arm, and an aromatic amine derivative of L-glutamic acid as a ligand. The binding capacities of the stationary phase were determined at different pH values (pH = 6, 7, and 8) using buffer solutions as mobile phase, and enantiomeric excess (ee) was determined by HPLC equipped with chiral column. The ee was found to be 47%. Chirality 22:252-257, 2010. (C) 2009 Wiley-Liss, Inc.</dc:description>
  <dc:identifier>https://aperta.ulakbim.gov.trrecord/26825</dc:identifier>
  <dc:identifier>oai:zenodo.org:26825</dc:identifier>
  <dc:rights>info:eu-repo/semantics/openAccess</dc:rights>
  <dc:rights>http://www.opendefinition.org/licenses/cc-by</dc:rights>
  <dc:source>CHIRALITY 22(2) 252-257</dc:source>
  <dc:title>Resolution of (+/-)-beta-Methylphenylethylamine by a Novel Chiral Stationary Phase for Pirkle-Type Column Chromatography</dc:title>
  <dc:type>info:eu-repo/semantics/article</dc:type>
  <dc:type>publication-article</dc:type>
</oai_dc:dc>
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