Dergi makalesi Açık Erişim
Yilmaz, Hayrullah; Topal, Giray; Cakmak, Resit; Hosgoren, Halil
{
"DOI": "10.1002/chir.20736",
"abstract": "In this study, a new Pirkle-type chiral column stationary phase for resolution of beta-methylphenylethyl amine was described by using activated Sepharose 4B as a matrix, L-tyrosine as a spacer arm, and an aromatic amine derivative of L-glutamic acid as a ligand. The binding capacities of the stationary phase were determined at different pH values (pH = 6, 7, and 8) using buffer solutions as mobile phase, and enantiomeric excess (ee) was determined by HPLC equipped with chiral column. The ee was found to be 47%. Chirality 22:252-257, 2010. (C) 2009 Wiley-Liss, Inc.",
"author": [
{
"family": "Yilmaz",
"given": " Hayrullah"
},
{
"family": "Topal",
"given": " Giray"
},
{
"family": "Cakmak",
"given": " Resit"
},
{
"family": "Hosgoren",
"given": " Halil"
}
],
"container_title": "CHIRALITY",
"id": "26825",
"issue": "2",
"issued": {
"date-parts": [
[
2010,
1,
1
]
]
},
"page": "252-257",
"title": "Resolution of (+/-)-beta-Methylphenylethylamine by a Novel Chiral Stationary Phase for Pirkle-Type Column Chromatography",
"type": "article-journal",
"volume": "22"
}
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