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Yilmaz, Hayrullah; Topal, Giray; Cakmak, Resit; Hosgoren, Halil
{ "DOI": "10.1002/chir.20736", "abstract": "In this study, a new Pirkle-type chiral column stationary phase for resolution of beta-methylphenylethyl amine was described by using activated Sepharose 4B as a matrix, L-tyrosine as a spacer arm, and an aromatic amine derivative of L-glutamic acid as a ligand. The binding capacities of the stationary phase were determined at different pH values (pH = 6, 7, and 8) using buffer solutions as mobile phase, and enantiomeric excess (ee) was determined by HPLC equipped with chiral column. The ee was found to be 47%. Chirality 22:252-257, 2010. (C) 2009 Wiley-Liss, Inc.", "author": [ { "family": "Yilmaz", "given": " Hayrullah" }, { "family": "Topal", "given": " Giray" }, { "family": "Cakmak", "given": " Resit" }, { "family": "Hosgoren", "given": " Halil" } ], "container_title": "CHIRALITY", "id": "26825", "issue": "2", "issued": { "date-parts": [ [ 2010, 1, 1 ] ] }, "page": "252-257", "title": "Resolution of (+/-)-beta-Methylphenylethylamine by a Novel Chiral Stationary Phase for Pirkle-Type Column Chromatography", "type": "article-journal", "volume": "22" }
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