1 Ocak 2010 Dergi makalesi Açık Erişim

Yilmaz, Hayrullah; Topal, Giray; Cakmak, Resit; Hosgoren, Halil

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  <identifier identifierType="URL">https://aperta.ulakbim.gov.tr/record/26825</identifier>
  <creators>
    <creator>
      <creatorName>Yilmaz, Hayrullah</creatorName>
      <givenName>Hayrullah</givenName>
      <familyName>Yilmaz</familyName>
      <affiliation>Dicle Univ, Fac Educ, Dept Chem, TR-21280 Diyarbakir, Turkey</affiliation>
    </creator>
    <creator>
      <creatorName>Topal, Giray</creatorName>
      <givenName>Giray</givenName>
      <familyName>Topal</familyName>
      <affiliation>Dicle Univ, Fac Educ, Dept Chem, TR-21280 Diyarbakir, Turkey</affiliation>
    </creator>
    <creator>
      <creatorName>Cakmak, Resit</creatorName>
      <givenName>Resit</givenName>
      <familyName>Cakmak</familyName>
      <affiliation>Dicle Univ, Fac Educ, Dept Chem, TR-21280 Diyarbakir, Turkey</affiliation>
    </creator>
    <creator>
      <creatorName>Hosgoren, Halil</creatorName>
      <givenName>Halil</givenName>
      <familyName>Hosgoren</familyName>
      <affiliation>Dicle Univ, Fac Sci &amp; Arts, Dept Chem, TR-21280 Diyarbakir, Turkey</affiliation>
    </creator>
  </creators>
  <titles>
    <title>Resolution Of (+/-)-Beta-Methylphenylethylamine By A Novel Chiral Stationary Phase For Pirkle-Type Column Chromatography</title>
  </titles>
  <publisher>Aperta</publisher>
  <publicationYear>2010</publicationYear>
  <dates>
    <date dateType="Issued">2010-01-01</date>
  </dates>
  <resourceType resourceTypeGeneral="Text">Journal article</resourceType>
  <alternateIdentifiers>
    <alternateIdentifier alternateIdentifierType="url">https://aperta.ulakbim.gov.tr/record/26825</alternateIdentifier>
  </alternateIdentifiers>
  <relatedIdentifiers>
    <relatedIdentifier relatedIdentifierType="DOI" relationType="IsIdenticalTo">10.1002/chir.20736</relatedIdentifier>
  </relatedIdentifiers>
  <rightsList>
    <rights rightsURI="http://www.opendefinition.org/licenses/cc-by">Creative Commons Attribution</rights>
    <rights rightsURI="info:eu-repo/semantics/openAccess">Open Access</rights>
  </rightsList>
  <descriptions>
    <description descriptionType="Abstract">In this study, a new Pirkle-type chiral column stationary phase for resolution of beta-methylphenylethyl amine was described by using activated Sepharose 4B as a matrix, L-tyrosine as a spacer arm, and an aromatic amine derivative of L-glutamic acid as a ligand. The binding capacities of the stationary phase were determined at different pH values (pH = 6, 7, and 8) using buffer solutions as mobile phase, and enantiomeric excess (ee) was determined by HPLC equipped with chiral column. The ee was found to be 47%. Chirality 22:252-257, 2010. (C) 2009 Wiley-Liss, Inc.</description>
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