1 Ocak 2013 Dergi makalesi Açık Erişim

Kilic, Ahmet; Palali, Ahmet Arif; Durgun, Mustafa; Tasci, Zeynep; Ulusoy, Mahmut; Dagdevren, Metin; Yilmaz, Ismail

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        "affiliation": "Harran Univ, Dept Chem, Sanliurfa, Turkey", 
        "name": "Kilic, Ahmet"
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      {
        "affiliation": "Harran Univ, Dept Chem, Sanliurfa, Turkey", 
        "name": "Palali, Ahmet Arif"
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      {
        "affiliation": "Harran Univ, Dept Chem, Sanliurfa, Turkey", 
        "name": "Durgun, Mustafa"
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      {
        "affiliation": "Mugla Univ, Dept Chem, TR-48000 Kotekli, Mugla, Turkey", 
        "name": "Tasci, Zeynep"
      }, 
      {
        "affiliation": "Harran Univ, Dept Chem, Sanliurfa, Turkey", 
        "name": "Ulusoy, Mahmut"
      }, 
      {
        "affiliation": "Istanbul Tech Univ, Dept Chem, TR-34469 Istanbul, Turkey", 
        "name": "Dagdevren, Metin"
      }, 
      {
        "affiliation": "Istanbul Tech Univ, Dept Chem, TR-34469 Istanbul, Turkey", 
        "name": "Yilmaz, Ismail"
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    "description": "Unsymmetrical dioxime ligand and its mono- and multinuclear metal complexes were synthesized and characterized by H-1 and C-13 NMR spectra, FT-IR, UV-Vis, elemental analysis, melting point measurements, LC-MS spectroscopy, molar conductivity measurements and magnetic susceptibility and cyclic voltammetry techniques. We firstly prepared new unsymmetrical dioxime ligand (1) and its mononuclear [Ni(dioxime)(2)] complex (2). Then, the intramolecular O-H center dot center dot center dot O bridges are replaced with Cu(II)(N-N) complex to synthesize multinuclear [Ni(dioxime)(2)Cu-2(N-N)(2)](ClO4)(2) oxime complexes (3-7) where N-N = 2,2'-bipyridine (bpy), 1,10-phenanthroline (phen), 3,3'-dicarboxy-2,2'-bipyridine (dcbpy), 4,5-diazafluoren-9-one (dafo) and 1,10-phenanthroline-5,6-dione (dione). The mononuclear complex [Ni(dioxime)(2)] (2) was used as a precursor for building multinuclear oxime complexes (3-7). In this paper, our goal is to study spectroscopic, electrochemical and catalytic properties of this new ligand and its metal complexes. (C) 2012 Elsevier B. V. All rights reserved.", 
    "doi": "10.1016/j.ica.2012.09.020", 
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    "journal": {
      "pages": "635-644", 
      "title": "INORGANICA CHIMICA ACTA", 
      "volume": "394"
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    "title": "Synthesis, characterization, electrochemical properties and conversions of carbon dioxide to cyclic carbonates mononuclear and multinuclear oxime complexes using as catalyst"
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