Dergi makalesi Açık Erişim
Goren, Ahmet C.; Sahin, Gozde; Gumilcineli, Ismail; Binici, Burcu
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"affiliation": "TUBITAK UME Natl Metrol Inst, Organ Chem Labs, TR-41470 Gebze, Turkey",
"name": "Goren, Ahmet C."
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"affiliation": "Zivak Technol, Gursel Mh Eski Besiktas Cad 44-1-2, TR-34400 Istanbul, Turkey",
"name": "Sahin, Gozde"
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"affiliation": "Zivak Technol, Gursel Mh Eski Besiktas Cad 44-1-2, TR-34400 Istanbul, Turkey",
"name": "Gumilcineli, Ismail"
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"description": "The 25-OH Vitamin D2 and 25-OH Vitamin D3 measurement method was validated using a Zivak Multitasker Fully Automated Sample Preparation and Injection System coupled to a MS detector. The current method incorporates all sample preparations, SPE clean up procedures, LC and MS facilities into an all in one system. This system can report patient data within 6 minutes including the SPE and Sample preparation and mass spectrometry analysis time. The correlation coefficient of the developed method was greater than 0.99 for measurands, 25-OH-vitamin Ds, in the calibration range. The measurement uncertainty of the measurements were evaluated and found as 7.7 % and 7.6 % for 25-OH vitamin D2 and 25-OH-vitamin D3, respectively.",
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"pages": "17-25",
"title": "JOURNAL OF CHEMICAL METROLOGY",
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"title": "Rapid and reliable 25-OH vitamin D2 and 25-OH vitamin D3 measurements by multitasker LC-MS/MS"
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