Dergi makalesi Açık Erişim
Goren, Ahmet C.; Sahin, Gozde; Gumilcineli, Ismail; Binici, Burcu
{
"DOI": "10.25135/jcm.13.18.02.070",
"abstract": "The 25-OH Vitamin D2 and 25-OH Vitamin D3 measurement method was validated using a Zivak Multitasker Fully Automated Sample Preparation and Injection System coupled to a MS detector. The current method incorporates all sample preparations, SPE clean up procedures, LC and MS facilities into an all in one system. This system can report patient data within 6 minutes including the SPE and Sample preparation and mass spectrometry analysis time. The correlation coefficient of the developed method was greater than 0.99 for measurands, 25-OH-vitamin Ds, in the calibration range. The measurement uncertainty of the measurements were evaluated and found as 7.7 % and 7.6 % for 25-OH vitamin D2 and 25-OH-vitamin D3, respectively.",
"author": [
{
"family": "Goren",
"given": " Ahmet C."
},
{
"family": "Sahin",
"given": " Gozde"
},
{
"family": "Gumilcineli",
"given": " Ismail"
},
{
"family": "Binici",
"given": " Burcu"
}
],
"container_title": "JOURNAL OF CHEMICAL METROLOGY",
"id": "93197",
"issue": "1",
"issued": {
"date-parts": [
[
2018,
1,
1
]
]
},
"page": "17-25",
"title": "Rapid and reliable 25-OH vitamin D2 and 25-OH vitamin D3 measurements by multitasker LC-MS/MS",
"type": "article-journal",
"volume": "12"
}
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