1 Ocak 2011 Dergi makalesi Açık Erişim

Kabay, Nilgun; Karadeniz, Hulya; Demirayak, Nuray; Gok, Yasar

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        "affiliation": "Pamukkale Univ, Dept Chem, TR-20017 Denizli, Turkey", 
        "name": "Kabay, Nilgun"
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      {
        "affiliation": "Council Forens Med, TR-61080 Trabzon, Turkey", 
        "name": "Karadeniz, Hulya"
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      {
        "affiliation": "Pamukkale Univ, Dept Chem, TR-20017 Denizli, Turkey", 
        "name": "Demirayak, Nuray"
      }, 
      {
        "affiliation": "Pamukkale Univ, Dept Chem, TR-20017 Denizli, Turkey", 
        "name": "Gok, Yasar"
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    "description": "The synthesis of new magnesium porphyrazines, peripherally substituted with 14-membered dioxa-dithia (O2S2) and tetrathia (S-4) macrocycles has been accomplished by cyclotetramerization of (6Z)-1,3,4,9,10,12-hexahydro-2,5,8,11-benzodioxadithia-cyclotetradecine-6,7-dicarbonitrile (3) or (62)-1,3,4,9,10,12-hexahydro-2,5,8,11-benzotetrathiacyclotetradecine-6,7-dicarbonitrile (5) in the presence of magnesium butanolate. The precursors were prepared from disodium salt of dithiomaleonitrile and o-xylenebis(1-chloro-3-oxapentane) (2) or o-xylenebis(1-chloro-3-thiapentane) (4). The metal-free porphyrazines are obtained by the treatment of these magnesium porphyrazines with trifluoroacetic acid. These new compounds are characterized by a combination of elemental analysis and H-1, C-13 NMR, IR, UV-vis and MS spectral data. Crown Copyright (C) 2011 Published by Elsevier B.V. All rights reserved.", 
    "doi": "10.1016/j.inoche.2011.01.039", 
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      "issue": "5", 
      "pages": "641-644", 
      "title": "INORGANIC CHEMISTRY COMMUNICATIONS", 
      "volume": "14"
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    "publication_date": "2011-01-01", 
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    "title": "Synthesis and characterization of new metallo and metal-free porphyrazines containing dioxadithia (O2S2) and tetrathia (S-4) macrocyclic moieties"
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