1 Ocak 2020 Dergi makalesi Açık Erişim

Karimi-Maleh, Hassan; Cellat, Kemal; Arikan, Kubilay; Savk, Aysun; Karimi, Fatemeh; Sen, Fatih

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    "creators": [
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        "name": "Karimi-Maleh, Hassan"
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      {
        "affiliation": "Dumlupinar Univ, Fac Arts & Sci, Dept Biochem, Sen Res Grp, Evliya Celebi Campus, TR-43100 Kutahya, Turkey", 
        "name": "Cellat, Kemal"
      }, 
      {
        "affiliation": "Dumlupinar Univ, Fac Arts & Sci, Dept Biochem, Sen Res Grp, Evliya Celebi Campus, TR-43100 Kutahya, Turkey", 
        "name": "Arikan, Kubilay"
      }, 
      {
        "affiliation": "Dumlupinar Univ, Fac Arts & Sci, Dept Biochem, Sen Res Grp, Evliya Celebi Campus, TR-43100 Kutahya, Turkey", 
        "name": "Savk, Aysun"
      }, 
      {
        "name": "Karimi, Fatemeh"
      }, 
      {
        "affiliation": "Dumlupinar Univ, Fac Arts & Sci, Dept Biochem, Sen Res Grp, Evliya Celebi Campus, TR-43100 Kutahya, Turkey", 
        "name": "Sen, Fatih"
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    "description": "In this study, we report the synthesis and application of palladium-nickel nanoparticles decorated on functionalized-multiwall carbon nanotube Pd-Ni@f-MWCNT and employed as a sensitive non-enzymatic electrochemical glucose sensor. The composition and crystal structure was characterized by X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD) and Raman spectroscopy. The surface morphology of Pd-Ni@f-MWCNT was investigated by a transmission electron microscopy (TEM). The electrochemical response of the Pd-Ni@f-MWCNT to glucose was examined via the cyclic voltammetry. Results revealed that the prepared electrode exhibits high electrocatalytic activity for the oxidation of glucose into gluconolactone. The ampero-metric response of the Pd-Ni@f-MWCNT electrode to glucose was investigated at a potential of 0.5 V that demonstrated an extended linear range of from 0.01 to 1.4 mM, very low detection limit of 0.026 mu M, very high sensitivity at 71 mu A mM(-1) cm(-2) , as well as good reproducibility, high stability and applicability for the real sample analysis. The reliability of the developed sensor was verified by comparison with a commercially available glucometer. The obtained results indicate that Pd-Ni@f-MWCNT is a promising candidate for electrochemical glucose sensing.", 
    "doi": "10.1016/j.matchemphys.2020.123042", 
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    "journal": {
      "title": "MATERIALS CHEMISTRY AND PHYSICS", 
      "volume": "250"
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    "publication_date": "2020-01-01", 
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    "title": "Palladium-Nickel nanoparticles decorated on Functionalized-MWCNT for high precision non-enzymatic glucose sensing"
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