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Karimi-Maleh, Hassan; Cellat, Kemal; Arikan, Kubilay; Savk, Aysun; Karimi, Fatemeh; Sen, Fatih
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<identifier identifierType="URL">https://aperta.ulakbim.gov.tr/record/11725</identifier>
<creators>
<creator>
<creatorName>Karimi-Maleh, Hassan</creatorName>
<givenName>Hassan</givenName>
<familyName>Karimi-Maleh</familyName>
</creator>
<creator>
<creatorName>Cellat, Kemal</creatorName>
<givenName>Kemal</givenName>
<familyName>Cellat</familyName>
<affiliation>Dumlupinar Univ, Fac Arts & Sci, Dept Biochem, Sen Res Grp, Evliya Celebi Campus, TR-43100 Kutahya, Turkey</affiliation>
</creator>
<creator>
<creatorName>Arikan, Kubilay</creatorName>
<givenName>Kubilay</givenName>
<familyName>Arikan</familyName>
<affiliation>Dumlupinar Univ, Fac Arts & Sci, Dept Biochem, Sen Res Grp, Evliya Celebi Campus, TR-43100 Kutahya, Turkey</affiliation>
</creator>
<creator>
<creatorName>Savk, Aysun</creatorName>
<givenName>Aysun</givenName>
<familyName>Savk</familyName>
<affiliation>Dumlupinar Univ, Fac Arts & Sci, Dept Biochem, Sen Res Grp, Evliya Celebi Campus, TR-43100 Kutahya, Turkey</affiliation>
</creator>
<creator>
<creatorName>Karimi, Fatemeh</creatorName>
<givenName>Fatemeh</givenName>
<familyName>Karimi</familyName>
</creator>
<creator>
<creatorName>Sen, Fatih</creatorName>
<givenName>Fatih</givenName>
<familyName>Sen</familyName>
<affiliation>Dumlupinar Univ, Fac Arts & Sci, Dept Biochem, Sen Res Grp, Evliya Celebi Campus, TR-43100 Kutahya, Turkey</affiliation>
</creator>
</creators>
<titles>
<title>Palladium-Nickel Nanoparticles Decorated On Functionalized-Mwcnt For High Precision Non-Enzymatic Glucose Sensing</title>
</titles>
<publisher>Aperta</publisher>
<publicationYear>2020</publicationYear>
<dates>
<date dateType="Issued">2020-01-01</date>
</dates>
<resourceType resourceTypeGeneral="Text">Journal article</resourceType>
<alternateIdentifiers>
<alternateIdentifier alternateIdentifierType="url">https://aperta.ulakbim.gov.tr/record/11725</alternateIdentifier>
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<relatedIdentifiers>
<relatedIdentifier relatedIdentifierType="DOI" relationType="IsIdenticalTo">10.1016/j.matchemphys.2020.123042</relatedIdentifier>
</relatedIdentifiers>
<rightsList>
<rights rightsURI="http://www.opendefinition.org/licenses/cc-by">Creative Commons Attribution</rights>
<rights rightsURI="info:eu-repo/semantics/openAccess">Open Access</rights>
</rightsList>
<descriptions>
<description descriptionType="Abstract">In this study, we report the synthesis and application of palladium-nickel nanoparticles decorated on functionalized-multiwall carbon nanotube Pd-Ni@f-MWCNT and employed as a sensitive non-enzymatic electrochemical glucose sensor. The composition and crystal structure was characterized by X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD) and Raman spectroscopy. The surface morphology of Pd-Ni@f-MWCNT was investigated by a transmission electron microscopy (TEM). The electrochemical response of the Pd-Ni@f-MWCNT to glucose was examined via the cyclic voltammetry. Results revealed that the prepared electrode exhibits high electrocatalytic activity for the oxidation of glucose into gluconolactone. The ampero-metric response of the Pd-Ni@f-MWCNT electrode to glucose was investigated at a potential of 0.5 V that demonstrated an extended linear range of from 0.01 to 1.4 mM, very low detection limit of 0.026 mu M, very high sensitivity at 71 mu A mM(-1) cm(-2) , as well as good reproducibility, high stability and applicability for the real sample analysis. The reliability of the developed sensor was verified by comparison with a commercially available glucometer. The obtained results indicate that Pd-Ni@f-MWCNT is a promising candidate for electrochemical glucose sensing.</description>
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