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Accurate determination of ethanol in water by qNMR: Validation and uncertainty assessment

Un, Ilker; Goren, Ahmet C.


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  <identifier identifierType="URL">https://aperta.ulakbim.gov.tr/record/97871</identifier>
  <creators>
    <creator>
      <creatorName>Un, Ilker</creatorName>
      <givenName>Ilker</givenName>
      <familyName>Un</familyName>
      <affiliation>UME, TUBITAK, P Box 54, TR-41470 Gebze, Turkey</affiliation>
    </creator>
    <creator>
      <creatorName>Goren, Ahmet C.</creatorName>
      <givenName>Ahmet C.</givenName>
      <familyName>Goren</familyName>
      <affiliation>UME, TUBITAK, P Box 54, TR-41470 Gebze, Turkey</affiliation>
    </creator>
  </creators>
  <titles>
    <title>Accurate Determination Of Ethanol In Water By Qnmr: Validation And Uncertainty Assessment</title>
  </titles>
  <publisher>Aperta</publisher>
  <publicationYear>2017</publicationYear>
  <dates>
    <date dateType="Issued">2017-01-01</date>
  </dates>
  <resourceType resourceTypeGeneral="Text">Journal article</resourceType>
  <alternateIdentifiers>
    <alternateIdentifier alternateIdentifierType="url">https://aperta.ulakbim.gov.tr/record/97871</alternateIdentifier>
  </alternateIdentifiers>
  <relatedIdentifiers>
    <relatedIdentifier relatedIdentifierType="DOI" relationType="IsIdenticalTo">10.25135/jcm.2.17.03.035</relatedIdentifier>
  </relatedIdentifiers>
  <rightsList>
    <rights rightsURI="http://www.opendefinition.org/licenses/cc-by">Creative Commons Attribution</rights>
    <rights rightsURI="info:eu-repo/semantics/openAccess">Open Access</rights>
  </rightsList>
  <descriptions>
    <description descriptionType="Abstract">A rapid and simple method, having high reproducibility and low uncertainty for determination of low concentration of ethanol in water has been developed by using qNMR. Method validation was performed applying CRM and calibration solutions. The correlation coefficient for the analyte in the calibration interval was 1. At a concentration range of 0.5 mg /g to 5 mg/g, the recovery was determined to be 99.71%. The relative uncertainties for ethanol solutions of 0.8123 mg/g and 3.8029 mg/g in water were found to be 0.0053 mg/g and 0.0027 mg/g, respectively.</description>
  </descriptions>
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