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Determination of sulfonamides in milk by ID-LC-MS/MS

Unsal, Isin Aydin; Tasan, Murat; Gokcen, Taner; Goren, Ahmet C.


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{
  "DOI": "10.25135/jcm.15.18.04.081", 
  "abstract": "In this study, an ID-LC-MS method was developed and validated for the determination of 14 sulfonamides in milk samples. Recovery results were found to be in the range of 91%-114% for milk samples. The relative measurement uncertainty was between 7.5%-12.7%. Validated method was performed on milk samples obtained from market and street vendors. The amount of sulfonamides in the analyzed samples was found to be below the legal limits (Sulfamethazine: 6.46 +/- 0.76 ng/g and sulfisoxazole: 7.3 +/- 0.71 ng/g).", 
  "author": [
    {
      "family": "Unsal", 
      "given": " Isin Aydin"
    }, 
    {
      "family": "Tasan", 
      "given": " Murat"
    }, 
    {
      "family": "Gokcen", 
      "given": " Taner"
    }, 
    {
      "family": "Goren", 
      "given": " Ahmet C."
    }
  ], 
  "container_title": "JOURNAL OF CHEMICAL METROLOGY", 
  "id": "93467", 
  "issue": "1", 
  "issued": {
    "date-parts": [
      [
        2018, 
        1, 
        1
      ]
    ]
  }, 
  "page": "70-78", 
  "title": "Determination of sulfonamides in milk by ID-LC-MS/MS", 
  "type": "article-journal", 
  "volume": "12"
}
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