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Topcu, Ezgi; Dagci, Kader; Alanyalioglu, Murat
<?xml version='1.0' encoding='utf-8'?> <resource xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xmlns="http://datacite.org/schema/kernel-4" xsi:schemaLocation="http://datacite.org/schema/kernel-4 http://schema.datacite.org/meta/kernel-4.1/metadata.xsd"> <identifier identifierType="URL">https://aperta.ulakbim.gov.tr/record/59015</identifier> <creators> <creator> <creatorName>Topcu, Ezgi</creatorName> <givenName>Ezgi</givenName> <familyName>Topcu</familyName> <affiliation>Ataturk Univ, Fac Sci, Dept Chem, TR-25240 Erzurum, Turkey</affiliation> </creator> <creator> <creatorName>Dagci, Kader</creatorName> <givenName>Kader</givenName> <familyName>Dagci</familyName> <affiliation>Ataturk Univ, Fac Sci, Dept Chem, TR-25240 Erzurum, Turkey</affiliation> </creator> <creator> <creatorName>Alanyalioglu, Murat</creatorName> <givenName>Murat</givenName> <familyName>Alanyalioglu</familyName> <affiliation>Ataturk Univ, Fac Sci, Dept Chem, TR-25240 Erzurum, Turkey</affiliation> </creator> </creators> <titles> <title>Free-Standing Graphene/Poly(Methylene Blue)/Agnps Composite Paper For Electrochemical Sensing Of Nadh</title> </titles> <publisher>Aperta</publisher> <publicationYear>2016</publicationYear> <dates> <date dateType="Issued">2016-01-01</date> </dates> <resourceType resourceTypeGeneral="Text">Journal article</resourceType> <alternateIdentifiers> <alternateIdentifier alternateIdentifierType="url">https://aperta.ulakbim.gov.tr/record/59015</alternateIdentifier> </alternateIdentifiers> <relatedIdentifiers> <relatedIdentifier relatedIdentifierType="DOI" relationType="IsIdenticalTo">10.1002/elan.201600108</relatedIdentifier> </relatedIdentifiers> <rightsList> <rights rightsURI="http://www.opendefinition.org/licenses/cc-by">Creative Commons Attribution</rights> <rights rightsURI="info:eu-repo/semantics/openAccess">Open Access</rights> </rightsList> <descriptions> <description descriptionType="Abstract">Highly flexible graphene/poly(methylene blue)/AgNPs composite paper was successfully prepared for amperometric biosensing of NADH. For this purpose, a dispersion including graphene oxide (GO), methylene blue (MB) and silver nanoparticles (AgNPs) was prepared and GO/MB/AgNPs paper was acquired by vacuum-filtration of this dispersion through a suitable membrane. After peeling it off from membrane, it was transformed to rGO/MB/AgNPs paper by performing reduction with hydriodic acid. In a three-electrode cell, which is containing 0.1M phosphate buffer solution (pH: 9.0), rGO/MB/AgNPs paper was used as working electrode and rGO/poly(MB)/AgNPs composite paper was generated by surface-confined electropolymerization of MB using successive cyclic voltammetry approach in a suitable potential window. Characterization of this composite paper was carried out by using scanning electron microscopy, scanning tunneling microscopy, X-ray photoelectron spectroscopy, powder X-ray diffraction spectroscopy, Raman spectroscopy, four-point probe conductivity measurement and cyclic voltammetry techniques. Flexible rGO/poly(MB)/AgNPs composite paper has demonstrated high sensitivity, wide linear range and low detection limit for amperometric quantification of NADH.</description> </descriptions> </resource>
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