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In-situ spark plasma sintering behavior of La2O3-Y2O3 co-doped AlON ceramics: An attempt to prevent carbon contamination

Aydogmus, Demet; Duygulu, Ozgur; Sahin, Filiz Cinar


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<oai_dc:dc xmlns:dc="http://purl.org/dc/elements/1.1/" xmlns:oai_dc="http://www.openarchives.org/OAI/2.0/oai_dc/" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.openarchives.org/OAI/2.0/oai_dc/ http://www.openarchives.org/OAI/2.0/oai_dc.xsd">
  <dc:creator>Aydogmus, Demet</dc:creator>
  <dc:creator>Duygulu, Ozgur</dc:creator>
  <dc:creator>Sahin, Filiz Cinar</dc:creator>
  <dc:date>2023-01-01</dc:date>
  <dc:description>Un-doped and La2O3-Y2O3 co-doped Aluminum oxynitride (AlON) ceramics were fabricated by reactive spark plasma sintering method (R-SPS) by using Al2O3 and AlN as starting powders with a composition of 70 mol% and 30 mol%, respectively. The effects of co doping system on densification, microstructure, mechanical properties and optical transmittance of AlON ceramics were investigated. X-ray analysis confirmed the fully transformation of g-AlON phase for all compositions prepared at 1650 degrees C in 30 min under 40 MPa under nitrogen. The results indicated that 0.02 wt% La2O3 thorn 0.08 wt% Y2O3 added composition had the optimal combination of sintering additives. In an attempt to reduce the graphite contamination, the powder mixture was encapsulated in a Nb-coated graphite foil before subjecting to SPS. Nb-coated graphite foil encapsulated sample was found to reduce carbon contamination leading to high densification (99.6 %) and high transmission (-81 % at 2500 nm). This study demonstrated that optical transmittance of R-SPSed AlON ceramics is significantly improved without any post-heat treatment by using Nb-coated graphite foil during SPS processing.(c) 2023 The Authors. Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).</dc:description>
  <dc:identifier>https://aperta.ulakbim.gov.trrecord/265104</dc:identifier>
  <dc:identifier>oai:aperta.ulakbim.gov.tr:265104</dc:identifier>
  <dc:rights>info:eu-repo/semantics/openAccess</dc:rights>
  <dc:rights>http://www.opendefinition.org/licenses/cc-by</dc:rights>
  <dc:source>JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&amp;T 27 13</dc:source>
  <dc:title>In-situ spark plasma sintering behavior of La2O3-Y2O3 co-doped AlON ceramics: An attempt to prevent carbon contamination</dc:title>
  <dc:type>info:eu-repo/semantics/article</dc:type>
  <dc:type>publication-article</dc:type>
</oai_dc:dc>
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