Yayınlanmış 1 Ocak 2011 | Sürüm v1
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Complete C-13 NMR assignments for ent-kaurane diterpenoids from Sideritis species

  • 1. Bogazici Univ, Dept Chem, TR-34342 Istanbul, Turkey
  • 2. Chem Grp Labs, TUBITAK UME, TR-41470 Gebze, Turkey
  • 3. Istanbul Univ, Fac Pharm, Dept Analyt Chem, TR-34116 Istanbul, Turkey
  • 4. Istanbul Tech Univ, Fac Sci & Letters, Dept Chem, TR-34469 Istanbul, Turkey

Açıklama

In this work, the detailed NMR studies and full C-13 NMR assignments for five diterpenoids isolated from Sideritis caesarea and Sideritis athoa are described. The assignments are based on a combination of 1D and 2D NMR techniques including H-1, C-13, H-1-H-1 COSY, gHSQC [(1)J(C,H)] and gHMBC delta(C) [(n)J(C,H) (n = 2 and 3)] and NOESY experiments. Copyright (C) 2011 John Wiley & Sons, Ltd.

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