Published January 1, 2013 | Version v1
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Full method validation for the determination of hexachlorobenzene and hexachlorobutadiene in fish tissue by GC-IDMS

  • 1. Commiss European Communities, Joint Res Ctr, IRMM, B-2440 Geel, Belgium
  • 2. TUBITAK Natl Metrol Inst, TR-41470 Gebze, Turkey

Description

This paper summarizes the validation strategy and the results obtained for the simultaneous determination of hexachlorobenzene (HCB) and hexachlorobutadiene (HCBD) in fish tissue with a maximum of about 10% m/m fat content using a GC-IDMS technique. The method is applicable for the determination of HCB and HCBD at trace levels in different kinds of fish tissue samples in accordance with the requirements of the EU Directive 2008/105/EC establishing Environmental Quality Standard (EQS) levels for biota in aquatic ecosystems (10 ng/g for HCB and 55 ng/g for HCBD).

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