Published January 1, 2015 | Version v1
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Microwave-assisted regioselective [1,3] -dipolar cycloaddition of 3-methyl-2-(substitutedbenzylidene)-5-oxopyrazolidin-2-ium-1-ides to benzothiophene 1,1-dioxide

  • 1. Abant Izzet Baysal Univ, Fac Arts & Sci, Dept Chem, Bolu, Turkey

Description

A series of pyrazolidinium ylides was reacted with benzothiophene 1,1-dioxide to afford (3R,5S,5aS,10bS)-3-methyl-5-substitutedphenyl-2,3,5,5a-tetrahydrobenzo [4,5] thieno [3,2-c] pyrazolo [1,2-a]pyrazol-1 (10bH)-one 6,6-dioxides under microwave irradiation and their structures were identified by means of spectral/physical characteristics including X-ray diffraction data and HRMS measurements.

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