Published January 1, 2016
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Modification of hexagonal boron nitride nanoparticles with fluorosilane
- 1. Akdeniz Univ, Dept Mech Engn, Dumlupinar Bulvari, TR-07058 Antalya, Turkey
- 2. Univ Cologne, Inst Inorgan Chem, Greinstr 6, D-50939 Cologne, Germany
- 3. Bilkent Univ UNAM, TR-06800 Ankara, Turkey
- 4. Akdeniz Univ, Fac Sci, Dept Chem, TR-07058 Antalya, Turkey
Description
Surfaces of hexagonal boron nitride (hBN) nanoparticles were modified with perfluorooctyl-triethoxysllane (FTS). Experiments were performed for 40-120 min in 70-150 degrees C range with FTS/hBN weight ratio in the range of 0.5-1.5. The products were analyzed by FT-IR, TGA, FESEM, HRTEM and EDX. Results of FT-IR analyses indicated that modification takes place in 80 min at 150 degrees C under reflux with a FTS/hBN ratio of 1.5. Presence of FTS on hBN nanoparticles was confirmed by the weight losses in TGA, and by TEM, TEM-EDX analyses. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
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