Published January 1, 2009
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Synthesis and Characterization of N-[1,10-Phenanthroline]-N '-[(Benzo-15-Crown-5)yl] Thiourea and Its Complex with Copper(I)
- 1. Yildiz Tech Univ, Fac Arts & Sci, Dept Chem, TR-34210 Esenler, Turkey
- 2. Tech Univ Istanbul, Dept Chem, Istanbul, Turkey
Description
A new thiourea ligand, N-[1,10-phenanthroline]-N'-[benzo-15-crown-5)yl]thiourea has been synthesized from the reaction of 5-amino-1,10-phenanthroline with 15-isothiocyanatobenzo[15-crown-5] and its Cu(I) complex has been prepared. The structures of the ligand and its complex have been characterized by elemental analysis, UV-vis, F-FIR, H-1 NMR (DMSO-d(6)), C-13 NMR (DMSO-d(6)) and MS spectra (LC-MS).
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