Yayınlanmış 1 Ocak 2018
| Sürüm v1
Dergi makalesi
Açık
Metathesis microwave synthesis, Rietveld refinement and optical studies of metal orthovanadates, MVO4 (M = Cr, Fe, Co, Ni, Cu)
Açıklama
Metathesis microwave synthesis (MMS) of metal orthovanadates (MNO4), M= Cr, Fe, Co, Ni, Cu) are realized with byproduct NaCl having high lattice energy driven in the forward direction of the MMS reaction based on ionic exchange The synthesis procedure is applied at 850 W powers in a domestic oven for a short time as 10 minutes The structural, morphological and optical properties of synthesized powders are determined by powder X-ray diffraction (XRD), Rietveld analysis, fourier transform infrared spectroscopy (FTIR), scanning electron microscopy/energy dispersive X-ray analysis and photoluminescence spectroscopy (PL) The unit cell parameters and crystal systems of the products are identified by Rietveld refinement method one by one.
Dosyalar
bib-3cfdb55c-e317-4424-a973-abe65494823e.txt
Dosyalar
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