Published January 1, 2010
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Synthesis and characterization of new air stable primary amido substituted diborane(4) derivatives
Creators
- 1. Adnan Menderes Univ, Dept Chem, TR-09010 Aydin, Turkey
- 2. Ondokuz Mayis Univ, Dept Phys, TR-55139 Samsun, Turkey
Description
Three new diborane(4) derivatives, 1,2-bis(2,4,6-trimethylanilide)-1,2-bis(dimethyamido)diborane(4) (1), 1,2-bis(2,4,6-trimethylanilide)-1,2-bis(duryl)diborane(4) (2) and 1,2-bis(anilide)-1,2-bis(duryl)diborane(4) (3), have been synthesized and characterized by means of elemental analysis, IR, H-1, DC and B-11 NMR spectroscopy. Additionally, the structures of compounds 1 and 2 have been determined by the single crystal X-ray diffraction technique. The compounds 1 and 2 crystallize in the monoclinic P21/c space group. All of the compounds were found to be air stable. (C) 2010 Elsevier Ltd. All rights reserved.
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