Published January 1, 2011
| Version v1
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Fast Method for Synthesis of Alkyl and Aryl-N-Methylnitrones
- 1. Gazi Univ, Fac Sci, Dept Chem, TR-06500 Ankara, Turkey
- 2. Cankiri Karatekin Univ, Fac Sci, Dept Chem, TR-18100 Cankiri, Turkey
- 3. Hitit Univ, Fac Sci & Arts, Dept Chem, TR-19030 Corum, Turkey
Description
A simple, fast, efficient and eco-friendly procedure was developed for the synthesis of alkyl and aryl-N-methylnitrones. The corresponding nitrones of aromatic aldehydes, aliphatic aldehydes and alicyclic carbonyl compounds were prepared from N-methylhydroxylamine hydrochloride and Na2CO3-Na2SO4 by simply grinding at room temperature without using solvent.
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