Published January 1, 2020
| Version v1
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Esterification of Fructose-oleic Acid by tert-Butanol/Dimethyl Sulfoxide and by 2-Methyl-2-butanol/Dimethyl Sulfoxide
Creators
- 1. Sivas Cumhuriyet Univ, Sci Fac, Dept Mol Biol & Genet, TR-58140 Sivas, Turkey
- 2. Europen Univ Lefke, Fac Pharm, Dept Pharmaceut Chem, TR-10 Mersin, Turkey
- 3. Sivas Cumhuriyet Univ, Dept Parasitol, Sch Med, TR-58140 Sivas, Turkey
- 4. Sci & Technol Res Council Turkey, Informat & Adv Technol Res Ctr Informat Secur, Analyt Instruments & Syst Dev Grp, Kocaeli, Turkey
Description
In this study two different strategy were followed to obtain a D-fructose-oleic acid ester. One of the strategies has been well established enzymatic synthesis of an ester bond. The other strategy excluded the biocatalyst and only used a mixture of two organic solvents as the reaction media, 2-methyl-2-butanol / dimethyl sulfoxide or tert-butanol / dimethyl sulfoxide for the production of D-fructose-oleic acid ester. Ester products obtained were characterised by using FT-IR, NMR, by MS. Product yield was also assessed by HPLC. Results of structural analyses and yield measurement indicated that two approaches produced almost identical ester products.
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